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Beilstein J. Org. Chem. 2014, 10, 1197–1212, doi:10.3762/bjoc.10.118
Graphical Abstract
Scheme 1: Formation of a dipeptide 3. Reaction of the amino group of amino acid 2 with the carboxylic acid mo...
Scheme 2: Peptide assembly by SPPS, exemplarily shown for a tetrapeptide. First, the C-terminal amino acid is...
Figure 1: Five issues that have to be resolved prior to peptide synthesis.
Scheme 3: Fmoc/t-Bu (A) and Boc/Bn (B) protecting-group strategies applied in SPPS. (A) The Fmoc-group is rem...
Figure 2: Commonly applied amino acid side chain protecting groups (SPG) in Fmoc/t-Bu-strategy. Trt: trityl, ...
Figure 3: Selected coupling reagents for SPPS.
Figure 4: Spectrum of methods for solid phase-synthesized peptides. AA: amino acid, SAR: structure–activity r...
Figure 5: Compounds that can be introduced into pNPY (porcine neuropeptide Y) or hPP (human pancreatic polype...